By Rutherford G. Montgomery
A Yankee Flier with the R.A.F. by way of Rutherford G. Montgomery
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This translates to less severe blue s h i f t i n g i n the o p t i c a l spectra. At the higher conversions, we have the case where the sample i s composed of a matrix of crosspolymerized material with small pockets of macromonomer. This would further decrease the a b i l i t y of the solvent to permeate the sample and make i t more d i f f i c u l t for the polydiacetylene chain to d i s t o r t since i t w i l l be locked into a network structure ( d i s t o r t i o n s would l i k e l y be limited to small changes such as s l i g h t torsions and bond angle deformations).
Thesis, Case Western Reserve University, Cleveland, Ohio. ; Campbell Smith, P. J . Acta. Cryst. 1978, A34, 3. ; Lando, J . B. I s . J . Chem. 1985, 25, 293. Havens, J . ; Thakur Macromolecules 1984 White, D. M. , , Polym Chem. 1971, 12(1), 155. Chance, R. ; Patel, G. ; Witt, J . D. J . Chem. Phys. 1979, 71, 206. Enkelmann, V. Advances i n Polymer Science 1984, 63, 91. ; L i e s e r , G. Macromolecules 1985, 18, 327. Hine, J . J . Org. Chem. 1966, 31, 1236. Thakur, M. ; Lando, J . B. accepted f o r publication i n Polymer.
2 Å. The reaction proceeds with a minimum of atomic and molecular motion (3). The reactive double bonds i n most of the topochemically polymeric crystals thus f a r found are related to the center of symmetry (centrosymmetric α-type c r y s t a l ) and dimerize to give highly c r y s t a l l i n e polymers containing cyclobutanes with a 1,3-trans configuration i n the main chain. A preparative study of four-center type photopolymerization has established the empirical rule that the c r y s t a l l i n e state [2+2] photodimerization of o l e f i n s can be widely extended to the c r y s t a l l i n e state photopolymerization of d i o l e f i n s with a r i g i d linear structure containing conjugated double bonds separated by the 1,4-position of an aromatic ring, such as s t i l b a z o l to DSP, or cinnamic derivatives to 1,4-phenylenediacrylic (p-PDA) derivatives (4).